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  • TT-AFM

    Atomic Force Microscope


    Producto Descontinuado u obsoleto



including a 15 or 50 Micron Scanner

This compact, tabletop Atomic Force Microscope has all the important features and benefits expected from a light lever AFM. The TT-AFM includes everything you need for AFM scanning: a stage, control electronics, probes, manuals, and a video microscope.

For:
Nanotechnology Researchers
Wanting to do routine scanning of nano-structures

Instrument Innovators
Using AFM as a platform to create a new instrument

Educators
Teaching students about AFM construction, operation, and applications

TT-AFM

 
Sample Sizes
up to 1” X 1” X 1/4”
 
Standard Scanning Modes
Vibrating, Non Vibrating, Phase, LFM
 
Scanners
50 X 50 X 17 microns, 15 X 15 X 7 microns
 
Video Optical Microscope
Zoom to 400X, 2 micron resolution
 
Stage and Ebox Size
Compact Tabletop Design
 
 

STAGE

The TT-AFM stage has excellent thermal and mechanical stability required for high resolution AFM scanning. Additionally, its open design facilitates user modification.

Rigid Frame Design The crossed beam design for the stage support is extremely rigid so the AFM is less susceptible to external vibrations.

Light Lever AFM Force Sensor Light lever force sensors are used in almost all atomic force microscopes and permit many types of experiments.

Integrated Probe Holder/Probe Exchanger A unique probe holder and clipping mechanism allows quick and easy probe exchange.

Direct Drive Z stage
A linear motion stage is used to move the probe in a perpendicular motion to the sample. Probe/sample angle alignment is not required, facilitating a much faster probe approach.

Small Footprint
The stage dimensions of 7.5 X 12” require little space and fit easily on a tabletop.

Precision XY Stage with Micrometer
The sample is moved relative to the probe with a precision xy micrometer stage. Thus, the sample can be moved without touching it.

Modes Electric Plug
A six pole electrical plug is located at the back of the stage to expand the capabilities of the TT-AFM.

XYZ Precision Piezo Scanner
The modified tripod design utilizes temperature compensated strain gauges which assure accurate measurements from images. Also, with this design it is possible to rapidly zoom into a feature visualized in an image.

Laser/Detector Alignment
Both the light lever laser and the photo detector adjustment mechanism may be directly viewed. This feature simplifies the laser/detector alignment.

Adaptable Sample Holder
At the top of the XYZ scanner is a removable cap that holds the sample. The cap can be modified - or a new cap can be designed – to hold many types of samples.

TT AFM

 

EBOX

Electronics in the TT-AFM are constructed around industry standard USB data acquisition electronics. The critical functions, such as xy scanning, are optimized with a 24 bit digital to analog converter. With the analog z feedback loop, the highest fidelity scanning is possible. Vibrating mode scanning is possible with both phase and amplitude feedback using the high sensitivity phase detection electronics.

24 bit scan DAC
Scanning waveforms for generating precision motion in the X-Y axis with the piezo scanners are created with 24 bit DACS driven by a 32 bit micro controller. With 24 bit scanning, the highest resolution AFM images may be measured. Feedback control using the xy strain gauges assures accurate tracking of the probe over the surface.

Phase and Amplitude Detector Circuit
Phase and amplitude in the Ebox are measured with highly stable phase and amplitude chips. The system can be configured to feed back on either phase or amplitude when scanning in vibrating mode.

Signal Accessible
At the rear of the eBox is a 50 pin ribbon cable that gives access to all of the primary electronic signals without having to open the eBox.

Status Lights
At the front of the Ebox is a light panel that has 7 lights. In the unlikely event of a circuit failure, these lights are used for determining the status of the Ebox power supplies.

Precision Analog Feedback
Feedback from the light lever force sensor to the Z piezoceramic is made using a precision analog feedback circuit. The position of the probe may be fixed in the vertical direction with a sample-and-hold circuit.

Variable Gain High Voltage Piezo Drivers
An improved signal to noise ratio, as well as extremely small scan ranges are possible with the variable gain high voltage piezo drivers.

EBOX

 

SOFTWARE

Software for acquiring images is designed with the industry standard LabView™ programming visual interface instrument design environment. There are many standard functions, including setting scanning parameters, probe approach, frequency tuning, and displaying images in real time. LabView™ facilitates rapid development for those users seeking to enhance the software with additional special features. LabView also enables the TT-AFM to be readily combined with any other instrument using LabView VI.

Pre-scan Window Pre-scan Window
A pre-scan window includes all of the functions that are required before a scan is started. The functions are presented in a logical sequence on the screen.
   
   
Scan Window Scan Window
Once all of the steps in the pre-scan window are completed, the scan window is used for measuring images. Scan parameter, Z feedback parameters, and image view functions may be changed with dialogs on this screen.
   
LabView Window LabView Window
Industry standard programming environment. Readily customized and modified for specialized applications. Instrumentation already using Labview can be added to the TT-AFM to create new capabilities.
 

IMAGE ANALYSIS SOFTWARE

Included with the TT-AFM is the Gwyddion open source SPM image analysis software. This complete image analysis package has all the software functions necessary to process, analyze and display SPM images.

IMAGE ANALYSIS SOFTWARE

  • visualization: false color representation with different types of mapping
  • shaded, logarithmic, gradient- and edge-detected, local contrast representation, Canny lines
  • OpenGL 3D data display: false color or material representation
  • easily editable color maps and OpenGL materials
  • basic operations: rotation, flipping, inversion, data arithmetic, crop, resampling
  • leveling: plane leveling, profiles leveling, three-point leveling, facet leveling, polynomial background removal, leveling along user-defined lines
  • value reading, distance and angle measurement
  • profiles: profile extraction, measuring distances in profile graph, profile export
  • filtering: mean, median, conservative denoise, Kuwahara, minimum, maximum, checker pattern removal
  • general convolution filter with user-defined kernel
  • statistical functions: Ra, RMS, projected and surface area, inclination, histograms, 1D and 2D correlation functions, PSDF, 1D and 2D angular distributions, Minkowski functionals, facet orientation analysis
  • statistical quantities calculated from area under arbitrary mask
  • row/column statistical quantities plots
  • ISO roughness parameter evaluation
  • grains: threshold marking and un-marking, watershed marking
  • grain statistics: overall and distributions of size, height, area, volume, boundary length, bounding dimensions
  • integral transforms: 2D FFT, 2D continuous wavelet transform (CWT), 2D discrete wavelet transform (DWT), wavelet anisotropy detection
  • fractal dimension analysis
  • data correction: spot remove, outlier marking, scar marking, several line correction methods (median, modus)
  • removal of data under arbitrary mask using Laplace or fractal interpolation
  • automatic xy plane rotation correction
  • arbitrary polynomial deformation on xy plane
  • 1D and 2D FFT filtering
  • fast scan axis drift correction
  • mask editing: adding, removing or intersecting with rectangles and ellipses, inversion, extraction, expansion, shrinking
  • simple graph function fitting, critical dimension determination
  • force-distance curve fitting
  • axes scale calibration
  • merging and immersion of images
  • tip modeling, blind estimation, dilation and erosion

 

 

VIDEO MICROSCOPE

A video optical microscope in an AFM serves three functions: aligning the laser onto the cantilever in the light lever AFM, locating surface features for scanning, and facilitating probe approach. The TT-AFM includes a high performance video optical microscope along with a 3 mega pixel ccd camera, light source, microscope stand, and Windows software for displaying images.

Video Microscope Video microscope used to locate surface features for scanning. The Vibrating Mode Cantilever is 125 μ long.
   
Video Microscope Laser alignment is greatly facilitated with the video optical microscope. This non-vibrating cantilever is 450 μ long. The red spot is from the laser reflecting off the cantilever.
 

PROBE HOLDER/EXCHANGE

The TT-AFM utilizes a unique probe holder/exchange mechanism. Probes are held in place with a spring device that mates with a probe exchange tool. With the probe exchange tool, changing probes takes only a few minutes.

PROBE HOLDER/EXCHANGE

 

TT-AFM IMAGES

With a vertical noise floor of 0.1 nm and a horizontal resolution of 2 nm, most types of samples may be imaged with the TT-AFM. These include hard as well as soft samples.

TT-AFM IMAGES

OPEN DESIGN

An open design is at the core of all products offered by the AFM Workshop. New types of experiments are more readily designed and implemented through the use of Lab View software. All the mechanical drawings for the TT-AFM are available in the documentation package option. Finally, the company’s website offers a Users Forum to directly share specialized designs developed for the TT-AFM. For specialized applications, other types of scanners such as flexure and tubes can be easily added to the microscope stage.

 

SCANNING MODES

Standard with every TT-AFM are non-vibrating(NV) mode and vibrating(V) modes for making topography scans. Additional modes included with the product are lateral force imaging as well as phase mode imaging. All of the scanning modes that can be implemented with a light lever AFM are possible with the TT-AFM.

With the window below, the resonance frequency of a cantilever is readily measured. Additionally, the phase characteristics of the probe sample interaction are captured.


Modes
 
Vibration Enclosure

TT-AFM OPTIONS

Although the TT-AFM comes with everything you need to make AFM images, several options are currently available.

Environmental Cell
Permits scanning in inert environments or liquids.

Scanner Fabrication Tool
Facilitates scanner fabrication.

High Resolution Scanner
Allows a range of 15 X 15 microns in XY and 7 microns in Z.

Vibration Cabinet
Reduces unwanted acoustic and structural vibrations.

Conductive AFM
Measures the 2-D conductivity of sample surfaces.

AFM Workshop regularly develops new Options. Contact AFM Workshop for more information on options for the TT-AFM.

Environmental Cell
 

SPECIFICATIONS


50 Micron xyz Scanner
Type Modified Tripod
xy Linearity < 1%
xy Range > 50 μ
xy Resolution < 10 nm closed loop
< 1 nm open loop
xy Actuator type Piezo
xy Sensor type Strain Gauge
z Range > 16 μ
z Linearity < 5 %
Z sensor noise < 5 nm
Z feedback noise < 0.2 nm*
Z Actuator Type Piezo
Z Sensor type Strain Gauge


15 Micron xyz Scanner
Type Modified tripod
XY Linearity < 1%
XY Range > 15 μ
XY resolution < 3 nm closed loop
< 0.3 nm open loop
XY Actuator type Piezo
Sensor type Strain Gauge
Z Range > 7 μ
Z Linearity < 5 %
Z sensor noise < 5 nm
Z feedback noise < 0.1 nm*
Z Actuator Type Piezo
Z Sensor type None

Sample Holder
Type Magnet
Max Lateral Dimensions 1 inch
Max. Height 0.25 inch
   Frequency 48 kHz

Light Lever AFM Force Sensor
Type Magnet
Probe Types Industry standard
Probe insertion Manual – probe
exchange tool
Probe holding mechanism Clip
Vibrating mode piezo
Electrical connector to probe
Laser/Detector adjustment range +/- 1.5 mm
Adjustment resolution 1 micron
Minimum Probe to Objective 25 mm
Laser Type 670 nm diode, < 5 mw
Detector  
   Type 4 quadrant
   Band Width > 500 kHz
   Signals Transmitted TL, BL, TR, BR
   Gain Lo, High Settings
Probe sample angle 10 degrees

Video Microscope 

 
Minimum Zoom
Maximum Zoom
 
Field of view
2 x 2 mm
300 x 300 u
 
Resolution
20 u
1.5u
 
Working Distance
114 mm
114 mm
 
Magnification
45X
400X
 


Software
Computer Industry Standard Computer

XY Translator
Range 25.4 mm
Resolution 2 μ
Type Bearing - spring loaded
Lock Down Yes


Z Motion
Type Direct Drive
Range 25 mm
Drive Type Stepper Motor
Min. Step Size 330 nm
Slew Rate 8 mm/minute
Limit Switch Top, Bottom
Control Software – rate, step size


Digital Data Input Output
Connection USB
Scanning DAC  
   Number 2
   Bits 24
   Frequency 7 kHz
Control DAC  
   Number 2
   Bits 14
   Frequency 2 kHz
ADC  
   Number 8
   Bits 14
   Frequency 48 kHz


Analog Electronics
   Freq Range 2 kHz – 800 kHz
   Output Voltage 10 Vpp
   Demod. Freq TBD
Z Feedback  
   Type PID
   Sample Hold Yes
   Voltage 0-150 V
XY Scan  
   Voltage 0 – 150 V
   Bandwidth > 200 Hz
   Pan & Zoom 22 Bits
Tip Approach Cutoff > 20 μ sec.


Software
Environment Lab View
Operating System Windows 7
Image Acquisition Real Time Display
(2 of 8 channels)
Control Parameters  
   PID Yes
   Setpoint Yes
   Range Yes
   Scan Rate Yes
   Image Rotate 0 and 90 degrees
Laser Align Yes
Vibrating Freq. Display Yes
Force Distance Yes
Tip Approach Yes
Oscilloscope Yes
Image Store Format Industry Standard
Image Pixels 16 X 16 to 1024 X 1024
H.V. Gain Control XY and Z
Real time display Line Level, Light Shaded,
Grey Color Pallet
Calibration System Window
Probe Center Yes




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